Microstructural evolution and mechanical properties of Mg alloys after processing by HPTE technique

Document Type : Research Article

Authors

Mechanical Engineering Department, Malayer University, Malayer, Iran

Abstract

This study investigates the effect of high-pressure torsion extrusion (HPTE) as a severe plastic deformation method on the mechanical properties and microstructure of AZ80 and ZK30 alloys. By inducing high strains, HPTE significantly improves the microstructure and mechanical properties of the samples. The alloys were initially produced by centrifugal casting and then subjected to HPTE at room temperature. Shear punch tests and Vickers hardness tests were conducted to assess mechanical properties, and the structure of the samples was examined using electron backscatter diffraction (EBSD). The average grain size of AZ80 alloy decreased from an initial value of 5.10 μm to 2.40 μm, 3.52 μm, and 3.33 μm for the v8ω0.6, v5ω1, and v1ω1 conditions, respectively. For ZK30 alloy, the grain size reduced from 30.87 μm to 6.51 μm under the v6ω0.6 condition. The final shear strength of AZ80 alloy in the extruded sample was 157 MPa, and under HPTE at the v8ω0.6 condition, it increased to 183 MPa. As the ω/v ratio increased, shear strength decreased. For ZK30 alloy, the shear strength in the extruded sample was 147 MPa, and under HPTE at the v6ω0.6 condition, it increased to 176 MPa, showing a 20% improvement. The results indicate that HPTE improves the mechanical properties of both alloys due to grain refinement during the process.

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Main Subjects


[1] T.G. Langdon, The processing of ultrafine-grained materials through the application of severe plastic deformation, Journal of Materials Science, 42 (2007) 3388-3397.
[2] G.F. Hesam Torabzadeh, A Review of Methods for Producing Ultrafine-Grained and Nanostructured Tubes via Severe Plastic Deformation (SPD, Modares Mechanical Engineering Journal, 16(6) (2016) 271-282., (in Persian).
[3] R.Z. Valiev, Y. Estrin, Z. Horita, T.G. Langdon, M.J. Zechetbauer, Y.T. Zhu, Producing bulk ultrafine-grained materials by severe plastic deformation, Jom, 58 (2006) 33-39.
[4] R.Z. Valiev, T.G. Langdon, Principles of equal-channel angular pressing as a processing tool for grain refinement, Progress in materials science, 51(7) (2006) 881-981.
[5] G.F. Armin Siah-Sarani, Farshad Samadpour, Structural and Mechanical Study of Magnesium Alloy Produced by Hydrostatic Extrusion-Expansion Severe Plastic Deformation Technique, Modares Journal of Mechanical Engineering, 20(4) (2020) 925-932.(in Persian).
[6] F.G. Dehghan Qods Effect of Reverse Accumulative Roll Bonding Process on the Microstructure, Mechanical Properties, and Property Heterogeneity of AA1050 Aluminum Alloy, Amirkabir Journal of Mechanical Engineering, 48(2) (2016) 197-206. (in Persian).
[7] S.H.G.G. Hamed Makhsoudloo Development of a Novel Lubrication System to Improve the Mechanical Properties of Ultrafine-Grained Titanium Produced by Hot Pressing in a Forward-Backward Rod-Extrusion Channel, Amirkabir Journal of Mechanical Engineering, 51(5) (2019) 1047-1056.(in Persian).
[8] G. Arhin, A.-b. Ma, J.-h. Jiang, E.K. Taylor, D. Song, Microstructure evolution and mechanical properties of Mg–Mn–RE alloy processed by equal channel angular pressing, Materials Today Communications, 38 (2024) 107744.
[9] S. Dai, M.A. Khan, L. Liao, X. Zhang, D. Zhao, H. Wang, M.A. Afifi, J. Li, Effect of hot extrusion, novel stepwise-rolling, and heat treatment on microstructure, mechanical properties, and precipitate chemistry of ultra-high strength Al-Zn-Mg-Cu alloy, Journal of Alloys and Compounds, 1010 (2025) 177910.
[10] S.Q. Khayavi Emadeddin, Plastic Deformation Behavior of Aluminum Alloy 5452 Disks Under Unconstrained High-Pressure Torsion Process and the Effect of Rotational Speed and Applied Pressures on Their Critical Radius, Iranian Journal of Manufacturing Engineering, 3(3) (2017) 40-47. (in Persian).
[11] Kohdar, Investigation of Microstructure and Pseudoelastic Behavior in Fe-10Ni-7Mn (wt.%) Alloy Before and After High-Pressure Torsion Process, Journal of Metallurgical Engineering, 24(3) (2021) 216-227.(in Persian).
[12] Y.T. Zhu, T.C. Lowe, T.G. Langdon, Performance and applications of nanostructured materials produced by severe plastic deformation, Scripta Materialia, 51(8) (2004) 825-830.
[13] K. Xue, Z. Luo, S. Xia, J. Dong, P. Li, Study of microstructural evolution, mechanical properties and plastic deformation behavior of Mg-Gd-Y-Zn-Zr alloy prepared by high-pressure torsion, Materials Science and Engineering: A, 891 (2024) 145953.
[14] Y. Ivanisenko, R. Kulagin, V. Fedorov, A. Mazilkin, T. Scherer, B. Baretzky, H. Hahn, High pressure torsion extrusion as a new severe plastic deformation process, Materials Science and Engineering: A, 664 (2016) 247-256.
[15] R.Z. Valiev, Y. Estrin, L.S. Toth, T.C. Lowe, Bulk nanostructured materials, Advanced Engineering Materials, 17(12, SI) (2015) 1708-1709.
[16] H. Höppel, M. Kautz, C. Xu, M. Murashkin, T. Langdon, R. Valiev, H. Mughrabi, An overview: Fatigue behaviour of ultrafine-grained metals and alloys, International Journal of Fatigue, 28(9) (2006) 1001-1010.
[17] K. Edalati, K. Imamura, T. Kiss, Z. Horita, Equal-channel angular pressing and high-pressure torsion of pure copper: Evolution of electrical conductivity and hardness with strain, Materials Transactions, 53(1) (2012) 123-127.
[18] A.Y. Khereddine, F.H. Larbi, M. Kawasaki, T. Baudin, D. Bradai, T.G. Langdon, An examination of microstructural evolution in a Cu–Ni–Si alloy processed by HPT and ECAP, Materials Science and Engineering: A, 576 (2013) 149-155.
[19] J. Li, F. Li, C. Zhao, H. Chen, X. Ma, J. Li, Experimental study on pure copper subjected to different severe plastic deformation modes, Materials Science and Engineering: A, 656 (2016) 142-150.
[20] B. Omranpour, L. Kommel, F. Sergejev, J. Ivanisenko, M. Antonov, M.A. Hernandez-Rodriguez, E. Garcia-Sanchez, Analysis of the reciprocal wear testing of Aluminum AA1050 processed by a novel mechanical nanostructuring technique, in:  IOP Conference Series: Materials Science and Engineering, IOP Publishing, 2021, pp. 012051.
[21] V. Tavakkoli, E. Boltynjuk, T. Scherer, A. Mazilkin, Y. Ivanisenko, T. Ungar, C. Kübel, Precipitate-mediated enhancement of mechanical and electrical properties in HPTE-processed Al–Mg–Si alloy, Materials Science and Engineering: A,  2024 pp. 146556.
[22] B. Omranpour, Y. Ivanisenko, R. Kulagin, L. Kommel, E.G. Sanchez, D. Nugmanov, T. Scherer, A. Heczel, J. Gubicza, Evolution of microstructure and hardness in aluminum processed by High Pressure Torsion Extrusion, Materials Science and Engineering: A, 762 (2019) 138074.
[23] D. Nugmanov, A. Mazilkin, H. Hahn, Y. Ivanisenko, Structure and tensile strength of pure Cu after high pressure torsion extrusion, Metals, 9(10) (2019) 1081.
[24] A. Bareggi, P. Boffi, S. Chinosi, S. Franchi Bononi, L. Guizzo, G. Lavecchia, M. Marzinotto, G. Mazzanti, G. Pozzati, Current and future applications of HPTE insulated cables systems, Cigrè Science & Engineering, 13 (2019) 34-44.
[25] E. Aghion, B. Bronfin, D. Eliezer, The role of the magnesium industry in protecting the environment, Journal of materials processing technology, 117(3) (2001) 381-385.
[26] D. Zhao, Z. Wang, M. Zuo, H. Geng, Effects of heat treatment on microstructure and mechanical properties of extruded AZ80 magnesium alloy, Materials & Design (1980-2015), 56 (2014) 589-593.
[27] T. Al-Samman, G. Gottstein, Room temperature formability of a magnesium AZ31 alloy: Examining the role of texture on the deformation mechanisms, Materials Science and Engineering: A, 488(1) (2008) 406-414.
[28] K. Kainer, F. Von Buch, The current state of technology and potential for further development of magnesium applications, Magnesium–alloys and technology,  2003 pp. 1-22.
[29] Y. Huang, R.B. Figueiredo, T. Baudin, F. Brisset, T.G. Langdon, Evolution of Strength and Homogeneity in a Magnesium AZ31 Alloy Processed by High‐Pressure Torsion at Different Temperatures, Advanced Engineering Materials, 14(11) (2012) 1018-1026.
[30] S.A. Alsubaie, P. Bazarnik, M. Lewandowska, Y. Huang, T.G. Langdon, Evolution of microstructure and hardness in an AZ80 magnesium alloy processed by high-pressure torsion, Journal of Materials Research and Technology, 5(2) (2016) 152-158.
[31] A. Al-Zubaydi, R.B. Figueiredo, Y. Huang, T.G. Langdon, Structural and hardness inhomogeneities in Mg–Al–Zn alloys processed by high-pressure torsion, Journal of Materials Science, 48 (2013) 4661-4670.
[32] G.M. Naik, S. Narendranath, S.S. Kumar, Effect of ECAP die angles on microstructure mechanical properties and corrosion behavior of AZ80 Mg alloy, Journal of Materials Engineering and Performance, 28 (2019) 2610-2619.
[33] S.A. Alsubaie, Y. Huang, T.G. Langdon, Hardness evolution of AZ80 magnesium alloy processed by HPT at different temperatures, Journal of Materials Research and Technology, 6(4) (2017) 378-384.